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Contents
1 Getting Started 3
1.1 Layout of the liquid handling system 3
1.2 Layout of the in situ sample stick 4
1.3 Layout of the pump 4
2 General procedures 6
2.1 Sample loading 6
2.1.1 Loading Vessel 1 6
2.1.2 Loading Vessel 2 6
2.2 Evacuation of the system 6
2.2.1 Removing air from Vessel 1 7
2.2.2 Removing air from Vessel 2 7
2.2.3 Removing air from Vessel 3 7
2.2.4 Evacuation of the sample cell 7
2.3 Freeze-Pump-Thaw cycle 8
2.3.1 Sample in Vessel 1 8
2.3.2 Sample in Vessel 2 8
2.3.3 Sample in Vessel 3 9
2.4 Liquid transfers 9
2.4.1 Vessel 1 to sample cell 9
2.4.2 Vessel 3 to sample cell 10
2.4.3 Recovery of liquid in manifold to Vessel 2 10
2.4.4 Recovery of liquid in sample cell to Vessel 1 11
2.4.5 Recovery of liquid in sample cell to Vessel 2 11
2.4.6 Recovery of liquid in sample cell to Vessel 3 11
3 Example Experiment 13
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